2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester

Base Information

Chemical Name:2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester
CAS No.:1489-55-0
Molecular Formula:C10H14O3
Molecular Weight:182.219
Hs Code.:
Mol file:1489-55-0.mol

Synonyms:Ethyl-3-methyl-6-keto-cyclohexen-3-carboxylat;1-Methyl-4-oxo-cyclohex-2-encarbonsaeure-aethylester;1-methyl-4-oxo-2-cyclohexene-1-carboxylic acid ethyl ester;4-Methyl-4-carbethoxycyclohex-2-enon;1-Methyl-cyclohexen-(2)-on-(4)-carbonsaeure-(1)-aethylester;1-Methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester;

Suppliers and Price of 2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 5 raw suppliers

Chemical Property of 2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester

Chemical Property:

Boiling Point:80-85 °C(Press: 0.3 Torr)
PSA：43.37000
Density:1.079±0.06 g/cm3(Predicted)
LogP:1.47490

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester

There total 6 articles about 2-Cyclohexene-1-carboxylic acid, 1-methyl-4-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1523-87-1
Ethyl 2-formyl-2-methyl-5-oxohexanoate

: 1489-55-0
1-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Guidance literature:: With piperidine; acetic acid; In tetrahydrofuran; at 20 ℃; for 24h; Heating / reflux;

Reference yield:

: 54843-13-9
3-hydroxy-2-methylacrylic acid ethyl ester

: 1489-55-0
1-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KOtBu / 2-methyl-propan-2-ol

2: piperidine acetate, AcOH / benzene

With potassium tert-butylate; piperdinium acetate; acetic acid; In tert-butyl alcohol; benzene;
DOI:10.1021/ja00814a022

Reference yield:

: 105-37-3,20741-13-3
Ethyl propionate

: 1489-55-0
1-methyl-4-oxo-cyclohex-2-enecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na / diethyl ether

2: KOtBu / 2-methyl-propan-2-ol

3: piperidine acetate, AcOH / benzene

With potassium tert-butylate; sodium; piperdinium acetate; acetic acid; In diethyl ether; tert-butyl alcohol; benzene;
DOI:10.1021/ja00814a022