4-benzyl-[1,4]thiazepane

Base Information

• Chemical Name: 4-benzyl-[1,4]thiazepane
• CAS No.: 71784-02-6
• Molecular Formula: C₁₂H₁₇NS
• Molecular Weight: 207.34
• Mol file: 71784-02-6.mol

Synonyms:

Chemical Property of 4-benzyl-[1,4]thiazepane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-benzyl-[1,4]thiazepane

There total 2 articles about 4-benzyl-[1,4]thiazepane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyl N-allyl amino-2 ethanethiol-1 (81829-66-5) → 4-benzyl-[1,4]thiazepane (71784-02-6) + 3-Benzyl-2-ethyl-thiazolidine (81829-71-2) + 4-Benzyl-2-methyl-thiomorpholine (81829-72-3)

Guidance literature:

With di-tert-butyl peroxide; In chlorobenzene; at 132 ℃; for 24h; Product distribution; irradiation, solvents, temperature; further N-allyl-2-aminothiols;

Reference yield:

→ 4-benzyl-[1,4]thiazepane (71784-02-6)

Guidance literature:

aus 2-Chlorethyl-3-chlorpropyl-sulfid (CLEPS), Benzylamin;

upstream raw materials:

N-benzyl N-allyl amino-2 ethanethiol-1

Refernces

• 1、 Strzelczyk,Kotelko. "Synthesis of hexahydro-1,4-thiazepine derivatives with expected pharmacological activity. Part I. N-alkyl(hydroxyalkyl)-hexahydro-1,4-thiazepines and 2-(hexahydro-1,4-thiazepinyl)-ethyl esters of phenoxy acetic acids". . p. 73 - 82,79,80,81. Retrieved 2007/10/05.