3H-1,2,4-Triazol-3-one, 5-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-[[2'-[2-(triphenylmethyl)-2H-tetr azol-5-yl][1,1'-biphenyl]-4-yl]methyl]-

Base Information

Chemical Name:3H-1,2,4-Triazol-3-one, 5-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-[[2'-[2-(triphenylmethyl)-2H-tetr azol-5-yl][1,1'-biphenyl]-4-yl]methyl]-
CAS No.:150312-86-0
Molecular Formula:C45H38ClN7O
Molecular Weight:728.296
Hs Code.:
Mol file:150312-86-0.mol

Synonyms:

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Chemical Property of 3H-1,2,4-Triazol-3-one, 5-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-[[2'-[2-(triphenylmethyl)-2H-tetr azol-5-yl][1,1'-biphenyl]-4-yl]methyl]-

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Technology Process of 3H-1,2,4-Triazol-3-one, 5-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-[[2'-[2-(triphenylmethyl)-2H-tetr azol-5-yl][1,1'-biphenyl]-4-yl]methyl]-

There total 3 articles about 3H-1,2,4-Triazol-3-one, 5-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-[[2'-[2-(triphenylmethyl)-2H-tetr azol-5-yl][1,1'-biphenyl]-4-yl]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 999-09-7
ethyl valerimidate

: 150312-86-0
5-n-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-<<2'-(N-trityltetrazol-5-yl)biphenyl-4-yl>methyl>-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

2: 2.) Et₃N / 1.) toluene, from 45 deg C to 50 deg C, 1.5 h, 2.) toluene, 90 deg C, overnight

3: 1.) NaH / 1.) DMF, from 40 deg C to 50 deg C, 20 min, 2.) DMF, 35 deg C, 2.5 h

With sodium hydride; triethylamine; In dichloromethane;
DOI:10.1021/jm00069a015

Reference yield:

: 83483-30-1
ethyl N-carbethoxyvalerimidate

: 150312-86-0
5-n-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-<<2'-(N-trityltetrazol-5-yl)biphenyl-4-yl>methyl>-3H-1,2,4-triazol-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) Et₃N / 1.) toluene, from 45 deg C to 50 deg C, 1.5 h, 2.) toluene, 90 deg C, overnight

2: 1.) NaH / 1.) DMF, from 40 deg C to 50 deg C, 20 min, 2.) DMF, 35 deg C, 2.5 h

With sodium hydride; triethylamine;
DOI:10.1021/jm00069a015

Reference yield:

: 133051-88-4
N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

: 133690-83-2
5-n-Butyl-2-(2-chlorophenyl)-2,4-dihydro-3H-1,2,4-triazol-3-one

: 150312-86-0
5-n-butyl-2-(2-chlorophenyl)-2,4-dihydro-4-<<2'-(N-trityltetrazol-5-yl)biphenyl-4-yl>methyl>-3H-1,2,4-triazol-3-one

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, from 40 deg C to 50 deg C, 20 min, 2.) DMF, 35 deg C, 2.5 h;
DOI:10.1021/jm00069a015