3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol

Base Information

Chemical Name:3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol
CAS No.:150809-46-4
Molecular Formula:C15H14O2
Molecular Weight:226.275
Hs Code.:
ChEMBL ID:CHEMBL3734936
DSSTox Substance ID:DTXSID601272113
Nikkaji Number:J1.649.892K
Mol file:150809-46-4.mol

Synonyms:SCHEMBL9419831;CHEMBL3734936;DTXSID601272113;150809-46-4;3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol

Suppliers and Price of 3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:226.099379685
Heavy Atom Count:17
Complexity:249

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=CC(=C1)C=CC2=CC(=CC=C2)O
Isomeric SMILES:COC1=CC=CC(=C1)/C=C/C2=CC(=CC=C2)O

Technology Process of 3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol

There total 5 articles about 3-[(1E)-2-(3-Methoxyphenyl)ethenyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 848487-57-0
(E)-1-methoxymethyloxy-3-(3-methoxy)styrylbenzene

: 150809-46-4
(E)-1-hydroxy-3-(3-methoxy)styrylbenzene

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; Heating;
DOI:10.1021/jm049238e

Reference yield:

: 874-98-6
1-bromomethyl-3-methoxybenzene

: 150809-46-4
(E)-1-hydroxy-3-(3-methoxy)styrylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 140 °C

2.1: NaOMe; 18/6-crown ether / dimethylformamide / 0.08 h / 20 °C

2.2: 95 percent / 18/6-crown ether / dimethylformamide / 6 h / 20 - 120 °C

3.1: 83 percent / pyridinium p-toluene sulfonate / methanol / Heating

With 18-crown-6 ether; sodium methylate; pyridinium p-toluenesulfonate; In methanol; N,N-dimethyl-formamide; 1.1: Arbuzov reaction / 2.2: Horner-Emmons-Wadsworth reaction;
DOI:10.1021/jm049238e

Reference yield:

: 13709-05-2
3-methoxymethoxybenzaldehyde

: 150809-46-4
(E)-1-hydroxy-3-(3-methoxy)styrylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOMe; 18/6-crown ether / dimethylformamide / 0.08 h / 20 °C

1.2: 95 percent / 18/6-crown ether / dimethylformamide / 6 h / 20 - 120 °C

2.1: 83 percent / pyridinium p-toluene sulfonate / methanol / Heating

With 18-crown-6 ether; sodium methylate; pyridinium p-toluenesulfonate; In methanol; N,N-dimethyl-formamide; 1.2: Horner-Emmons-Wadsworth reaction;
DOI:10.1021/jm049238e