α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid

Base Information

• Chemical Name: α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid
• CAS No.: 1719-28-4
• Molecular Formula: C₂₈H₃₂N₂O₇
• Molecular Weight: 508.571

Synonyms:

Chemical Property of α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid

There total 3 articles about α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-α-amino-m,p-dimethoxyphenylacetic acid (91819-11-3) → α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid (1719-28-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH

2: (i) PCl₅, (ii) /BRN= 474393/

With sodium hydroxide;

DOI:10.1039/jr9650003645

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid (1719-28-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH

2: (i) PCl₅, (ii) /BRN= 474393/

With sodium hydroxide;

DOI:10.1039/jr9650003645

Reference yield:

N-Benzyloxycarbonyl-α-<3,4-dimethoxy-phenyl>-glycin (1719-27-3) + 2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) → α--3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid (1719-28-4)

Guidance literature:

Multistep reaction; (i) PCl₅, (ii) /BRN= 474393/;

DOI:10.1039/jr9650003645

upstream raw materials:

N-Benzyloxycarbonyl-α-<3,4-dimethoxy-phenyl>-glycin

2-(3,4-dimethoxyphenyl)-ethylamine

D-α-amino-m,p-dimethoxyphenylacetic acid

benzyl chloroformate

Downstream raw materials:

α-Formamido-3,4-dimethoxy-N-<3,4-dimethoxy-phenethyl>-phenylacetamid

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