Ethanethiol, 2,2'-[(phenylmethyl)imino]bis-

Base Information

• Chemical Name: Ethanethiol, 2,2'-[(phenylmethyl)imino]bis-
• CAS No.: 1517-91-5
• Molecular Formula: C11H17NS2
• Molecular Weight: 227.395
• Mol file: 1517-91-5.mol

Synonyms:

Chemical Property of Ethanethiol, 2,2'-[(phenylmethyl)imino]bis-

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethanethiol, 2,2'-[(phenylmethyl)imino]bis-

There total 2 articles about Ethanethiol, 2,2'-[(phenylmethyl)imino]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

thirane (420-12-2) + benzylamine (100-46-9) → 2-[benzyl(2-mercaptoethyl)amino]ethanethiol (1517-91-5)

Guidance literature:

In toluene; at 20 - 80 ℃; for 10h;

DOI:10.1021/jm000050e

Reference yield:

→ 2-[benzyl(2-mercaptoethyl)amino]ethanethiol (1517-91-5)

Guidance literature:

PhCH2N(CH2CH2-S-C(=NH)NH2)2, NaOH, H2O;

Reference yield: 68.0%

bis(acetylacetonato)dioxomolybdenum(VI) + 2-[benzyl(2-mercaptoethyl)amino]ethanethiol (1517-91-5) → [MoO2(benzylbis(2-mercaptoethyl)amine-2H)] (827307-18-6)

Guidance literature:

In methanol; under N2; soln. of amine in methanol added to soln. of Mo-complex in methanol at 60°C, mixt. heated for 30 min; solid filtered off, washed with methanol, diethyl ether and hexane, dried under vac.; elem. anal.;

DOI:10.1016/j.ica.2004.07.008

upstream raw materials:

thirane

benzylamine

Downstream raw materials:

[MoO₂(benzylbis(2-mercaptoethyl)amine-2H)]