[Ni₂S(SC₃H₇)(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)*C₄H₈O=[Ni₂S(SC₃H₇)(C₆H₁₄PCH₂CH₂PC₆H₁₄)2]B(C₆H₅)4*C₄H₈O

Base Information

• Chemical Name: [Ni₂S(SC₃H₇)(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)*C₄H₈O=[Ni₂S(SC₃H₇)(C₆H₁₄PCH₂CH₂PC₆H₁₄)2]B(C₆H₅)4*C₄H₈O
• CAS No.: 437987-41-2
• Molecular Formula: C₄H₈O*C₂₄H₂₀B*C₃₁H₇₁Ni₂P₄S₂
• Molecular Weight: 1140.65
• Mol file: 437987-41-2.mol

Synonyms:

Chemical Property of [Ni₂S(SC₃H₇)(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)*C₄H₈O=[Ni₂S(SC₃H₇)(C₆H₁₄PCH₂CH₂PC₆H₁₄)2]B(C₆H₅)4*C₄H₈O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Ni₂S(SC₃H₇)(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)*C₄H₈O=[Ni₂S(SC₃H₇)(C₆H₁₄PCH₂CH₂PC₆H₁₄)2]B(C₆H₅)4*C₄H₈O

There total 1 articles about [Ni₂S(SC₃H₇)(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)*C₄H₈O=[Ni₂S(SC₃H₇)(C₆H₁₄PCH₂CH₂PC₆H₁₄)2]B(C₆H₅)4*C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + Ni2S2(((CH3)2CH)2PCH2CH2P(CH(CH3)2)2)2 (223525-66-4) + toluene-4-sulfonic acid isopropyl ester (2307-69-9) + sodium tetraphenyl borate (143-66-8) → [Ni2S(SC3H7)(((CH3)2CH)2PCH2CH2P(CH(CH3)2)2)2](1+)*B(C6H5)4(1-)*C4H8O=[Ni2S(SC3H7)(C6H14PCH2CH2PC6H14)2]B(C6H5)4*C4H8O (437987-41-2)

Guidance literature:

In tetrahydrofuran; (N2); addn. of a soln. of ligand in THF to a soln. of nickel complex in THF, stirring for 3 d, evapn., dissolving in THF, layering with hexanes,cooling at -30°C, dissolving in THF, addn. of boron compd., stir ring overnight; filtration through Al2O3, evapn.;

DOI:10.1016/S0020-1693(01)00770-8

upstream raw materials:

tetrahydrofuran

Ni₂S₂(((CH₃)2CH)2PCH₂CH₂P(CH(CH₃)2)2)2

toluene-4-sulfonic acid isopropyl ester

sodium tetraphenyl borate