Technology Process of 6-Hydroxybenzbromarone
There total 7 articles about 6-Hydroxybenzbromarone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride; ethanethiol;
In
dichloromethane;
for 1.5h;
Cooling with ice/NaCl bath;
DOI:10.1021/jm1015022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tin(IV) chloride / carbon disulfide / 5 - 20 °C / Inert atmosphere; Cooling with ice
2: sodium thioethylate / N,N-dimethyl-formamide / 1 h / 105 - 110 °C
3: N-Bromosuccinimide / dichloromethane; N,N-dimethyl-formamide / 20 h / 20 °C / Cooling with ice-brine bath
4: aluminum (III) chloride; ethanethiol / dichloromethane / 1.5 h / Cooling with ice/NaCl bath
With
aluminum (III) chloride; N-Bromosuccinimide; tin(IV) chloride; ethanethiol; sodium thioethylate;
In
carbon disulfide; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm1015022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium thioethylate / N,N-dimethyl-formamide / 1 h / 105 - 110 °C
2: N-Bromosuccinimide / dichloromethane; N,N-dimethyl-formamide / 20 h / 20 °C / Cooling with ice-brine bath
3: aluminum (III) chloride; ethanethiol / dichloromethane / 1.5 h / Cooling with ice/NaCl bath
With
aluminum (III) chloride; N-Bromosuccinimide; ethanethiol; sodium thioethylate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm1015022
