10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide

Base Information

Chemical Name:10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide
CAS No.:15320-91-9
Molecular Formula:C14H13O3P
Molecular Weight:260.229
Hs Code.:
NSC Number:666503,129497
DSSTox Substance ID:DTXSID90299340
Nikkaji Number:J1.222.925I
Wikidata:Q82041680
ChEMBL ID:CHEMBL1896431
Mol file:15320-91-9.mol

Synonyms:NSC666503;15320-91-9;MLS002707381;10-hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide;2,8-Dimethyl-10H-phenoxaphosphin-10-ol 10-oxide;CHEMBL1896431;SCHEMBL19091717;DTXSID90299340;NSC129497;NSC-129497;NSC-666503;SMR001574772;10-hydroxy-2,8-dimethyl-phenoxaphosphinine 10-oxide;10-hydroxy-2,8-dimethyl-10h-10lambda5-phenoxaphosphine 10-oxide

Suppliers and Price of 10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide

Chemical Property:

Vapor Pressure:1.63E-11mmHg at 25°C
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:260.06023127
Heavy Atom Count:18
Complexity:340

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)OC3=C(P2(=O)O)C=C(C=C3)C

Technology Process of 10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide

There total 6 articles about 10-Hydroxy-2,8-dimethylphenoxaphosphinine 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.2%

: 1579-40-4
1,1'-oxybis(4-methyl-benzene)

: 15320-91-9
2,8-Dimethyl-5-hydroxy-5-oxo-P^v-dibenzo<1,4>oxaphosphorin

Guidance literature:: 1,1'-oxybis(4-methyl-benzene); With aluminium trichloride; phosphorus trichloride; Heating;

With sodium hydroxide; dihydrogen peroxide; In water; for 0.25h;
DOI:10.1021/jo0300183

Reference yield: 92.0%

: 21990-64-7
2,8-dimethyl-10H-10λ⁵-phenoxaphosphine 10-oxide

: 15320-91-9
2,8-Dimethyl-5-hydroxy-5-oxo-P^v-dibenzo<1,4>oxaphosphorin

Guidance literature:: With potassium hydroxide; oxygen; In water;
DOI:10.1007/s11172-005-0209-4

Reference yield:

: 65654-60-6
(10-chloro-2,8-dimethyl-10H-phenoxaphosphine)

: 15320-91-9
2,8-Dimethyl-5-hydroxy-5-oxo-P^v-dibenzo<1,4>oxaphosphorin

Guidance literature:: Multi-step reaction with 2 steps

1: 10.2 g / H₂O / 0 °C

2: 92 percent / O₂; KOH / H₂O

With potassium hydroxide; water; oxygen; In water;
DOI:10.1007/s11172-005-0209-4