(N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾

Base Information

Chemical Name:(N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾
CAS No.:126130-92-5
Molecular Formula:C₂₅H₁₉CrNO₅S
Molecular Weight:497.492
Hs Code.:

(N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium<sup>(0)</sup>

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Chemical Property of (N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾

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Technology Process of (N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾

There total 1 articles about (N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15038-41-2
pentacarbonyl(tetrahydrofuran)chromium⁽⁰⁾

: 60140-96-7
N,N-dibenzyl benzenesulfenamide

: 126130-92-5
(N,N-dibenzyl)benzene sulfenamide pentacarbonylchromium⁽⁰⁾

Guidance literature:: In tetrahydrofuran; byproducts: THF; a soln. of sulfenamide in THF is added to Cr(CO)5*THF, the mixt. is stirred for 60 min. (reaction is performed under an oxygen-free nitrogen atmosphere); removal of solvent under reduced pressure, the excess of hexacarbonyl is vac. sublimed at room. temp., the residue is redissolved in n-hexane, filtered through kieselguhr and cooled at -30°C for 12 h, elem. anal.;