1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]-

Base Information

Chemical Name:1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]-
CAS No.:154081-22-8
Molecular Formula:C11H13BO2
Molecular Weight:188.034
Hs Code.:
Mol file:154081-22-8.mol

Synonyms:2-[(E)-styryl]-1,3,2-dioxaborinane;1,3,2-Dioxaborinane,2-[(1E)-2-phenylethenyl];(E)-styrylboronic acid 1,3-propandiol ester;

Suppliers and Price of 1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]-

Chemical Property:

PSA：18.46000
LogP:2.16410

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]-

There total 3 articles about 1,3,2-Dioxaborinane, 2-[(1E)-2-phenylethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6783-05-7
trans-2-phenylvinylboronic acid

: 504-63-2
trimethyleneglycol

: 154081-22-8
(E)-styrylboronic acid 1,3-propandiol ester

Guidance literature:: With magnesium sulfate; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jacs.8b10769

Reference yield: 85.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 5,5--dimethyl--2--vinyl-1,3,2-dioxaborinane

: 154081-22-8
(E)-styrylboronic acid 1,3-propandiol ester

: 588-59-0
stilbene

Guidance literature:: carbonylchlorohydridobis(tricyclohexylphosphine)ruthenium(II); In dichloromethane; at 40 ℃; for 3h;
DOI:10.1039/b414644a

Reference yield: 85.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 5,5--dimethyl--2--vinyl-1,3,2-dioxaborinane

: 154081-22-8
(E)-styrylboronic acid 1,3-propandiol ester

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; byproducts: C6H5C2H2C6H5; in CH2Cl2 (vinylborane:olefin=1:1), with Ru complex, at 40°C for 3 h; MAS;
DOI:10.1039/b414644a