9,10-Difluoroanthracene

Base Information

Chemical Name:9,10-Difluoroanthracene
CAS No.:1545-69-3
Molecular Formula:C14H8F2
Molecular Weight:214.214
Hs Code.:
Mol file:1545-69-3.mol

Synonyms:9,10-Difluoranthracen;9,10-difluoro-anthracene;9,10-Difluoroanthracen;9,10-Difluor-anthracen;

Suppliers and Price of 9,10-Difluoroanthracene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of 9,10-Difluoroanthracene

Chemical Property:

PSA：0.00000
LogP:4.27120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9,10-Difluoroanthracene

There total 9 articles about 9,10-Difluoroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 120-12-7
anthracene

: 1545-69-3
9,10-Difluoroanthracene

: 529-85-1
9-fluoroantracene

Guidance literature:: With N-fluoropyridinium triflate; In 1,2-dichloro-ethane; for 5h; Heating;
DOI:10.1021/jo00266a006

Reference yield:

: 13387-47-8
9,10-di-tert-butyl-9,10-dihydroanthracene

: 1545-69-3
9,10-Difluoroanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / DDQ / benzene / 14 h / 140 °C

2: 24 percent / N-fluoropyridinium triflate ⁽³³⁾ / 1,2-dichloro-ethane / 5 h / Heating

With N-fluoropyridinium triflate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,2-dichloro-ethane; benzene;
DOI:10.1021/jo00266a006

Reference yield:

: 523-27-3
9,10-Dibromoanthracene

: 1545-69-3
9,10-Difluoroanthracene

Guidance literature:: With n-butyllithium; N-fluoro-N-(tert-butyl)benzenesulfonamide; Yield given. Multistep reaction; 1.) ether, 10 min, 2.) ether, from -78 deg C to RT;
DOI:10.1021/jo00244a056