La(C₆H₅C₃N₂(CH₃)2ONHCOCH₃)2Br₃

Base Information

• Chemical Name: La(C₆H₅C₃N₂(CH₃)2ONHCOCH₃)2Br₃
• CAS No.: 121461-93-6
• Molecular Formula: C₂₆H₃₀Br₃LaN₆O₄
• Molecular Weight: 869.18
• Mol file: 121461-93-6.mol

Synonyms:

Chemical Property of La(C₆H₅C₃N₂(CH₃)2ONHCOCH₃)2Br₃

Chemical Property:

Purity/Quality:

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Technology Process of La(C₆H₅C₃N₂(CH₃)2ONHCOCH₃)2Br₃

There total 1 articles about La(C₆H₅C₃N₂(CH₃)2ONHCOCH₃)2Br₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetylaminoantipyrine (83-15-8) + lanthanum(III) bromide (13536-79-3) → La(C6H5C3N2(CH3)2ONHCOCH3)2Br3 (121461-93-6)

Guidance literature:

In ethanol; a soln. of LaBr3 is refluxed with a soln. of the ligand (1:3) both in ethanol on a waterbath for about 1 h; sepn. of the complex by standing or removing the solvent by concn.; cooling to room temp.; collecting the product; washing with cold ethanol, finally with ether; drying in vacuo over P2O5; elem. anal.;

upstream raw materials:

4-acetylaminoantipyrine

lanthanum(III) bromide

Refernces