azido(trioctyl)stannane

Base Information

• Chemical Name: azido(trioctyl)stannane
• CAS No.: 154704-56-0
• Molecular Formula: C24H51N3Sn
• Mol file: 154704-56-0.mol

Synonyms:

Chemical Property of azido(trioctyl)stannane

Chemical Property:

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of azido(trioctyl)stannane

There total 6 articles about azido(trioctyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

trioctyltin chloride (2587-76-0) → tri-n-octyltin azide (154704-56-0)

Guidance literature:

With sodium azide; In water; at 20 ℃; for 5h; Cooling;

Reference yield:

aqueous sodium chloride + trioctyltin chloride (2587-76-0) → trioctyltin azide (154704-56-0)

Guidance literature:

In water;

Reference yield:

octylmagnesium bromide (17049-49-9) → tri-n-octyltin azide (154704-56-0)

Guidance literature:

Multi-step reaction with 4 steps

1: n-heptane; diethyl ether / 0 - 20 °C / Inert atmosphere

2: iodine / methanol / 60 °C / Reflux

3: hydrogenchloride / n-heptane; water / 0.5 h / 20 °C

4: sodium azide / water / 5 h / 20 °C / Cooling

With hydrogenchloride; sodium azide; iodine; In methanol; diethyl ether; n-heptane; water;

upstream raw materials:

trioctyltin chloride

octylmagnesium bromide

tri-n-octyl(phenyl)stannane

trioctyltin acetate