N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate

Base Information

• Chemical Name: N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate
• CAS No.: 123843-34-5
• Molecular Formula: C₁₈H₃₉NOSb*C₂₄H₂₀B
• Molecular Weight: 726.498
• Mol file: 123843-34-5.mol

Synonyms:

Chemical Property of N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate

There total 1 articles about N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-N,N-diethylacetamide (2430-01-5) + sodium tetraphenyl borate (143-66-8) + tributylstibine (2155-73-9) → N,N-diethylaminocarbonylmethyltri-n-butylstibonium tetraphenylborate (123843-34-5)

Guidance literature:

In ethanol; (C4H9)3Sb and N,N-diethyl bromoacetamide are placed in a vessel, which then is flushed with N2, mixt. is stirred at room temp for 8 h, C2H5OH is added, stirred at room temp., mixt. is added to a soln. of NaBPh4.; White solid is recrystd. from ether, elem. anal.;

DOI:10.1016/0022-328X(89)87318-8

upstream raw materials:

2-bromo-N,N-diethylacetamide

sodium tetraphenyl borate

tributylstibine

Refernces