Carbamic acid, [1-[(1-formyl-1H-indol-3-yl)methyl]-2-[methyl(phenylmethyl)amino]-2-oxo ethyl]-, 1,1-dimethylethyl ester, (S)-

Base Information

Chemical Name:Carbamic acid, [1-[(1-formyl-1H-indol-3-yl)methyl]-2-[methyl(phenylmethyl)amino]-2-oxo ethyl]-, 1,1-dimethylethyl ester, (S)-
CAS No.:154812-36-9
Molecular Formula:C₂₅H₂₉N₃O₄
Molecular Weight:435.523
Hs Code.:
Mol file:154812-36-9.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [1-[(1-formyl-1H-indol-3-yl)methyl]-2-[methyl(phenylmethyl)amino]-2-oxo ethyl]-, 1,1-dimethylethyl ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [1-[(1-formyl-1H-indol-3-yl)methyl]-2-[methyl(phenylmethyl)amino]-2-oxo ethyl]-, 1,1-dimethylethyl ester, (S)-

There total 1 articles about Carbamic acid, [1-[(1-formyl-1H-indol-3-yl)methyl]-2-[methyl(phenylmethyl)amino]-2-oxo ethyl]-, 1,1-dimethylethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 47355-10-2
Nα-tert-butoxycarbonyl-1-formyl-L-tryptophan

: 103-67-3
benzyl-methyl-amine

: 154812-36-9
[(S)-1-(Benzyl-methyl-carbamoyl)-2-(1-formyl-1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With WSCD*HCl; benzotriazol-1-ol; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00039a022

Reference yield:

: 154812-36-9
[(S)-1-(Benzyl-methyl-carbamoyl)-2-(1-formyl-1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

: (S)-2-Amino-N-benzyl-3-(1-formyl-1H-indol-3-yl)-N-methyl-propionamide; hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; Ambient temperature;
DOI:10.1021/jm00039a022

Reference yield:

: 154812-36-9
[(S)-1-(Benzyl-methyl-carbamoyl)-2-(1-formyl-1H-indol-3-yl)-ethyl]-carbamic acid tert-butyl ester

: 158574-82-4
<(1-methyl-1H-indol-3-yl)carbonyl>-(2S,4R)Hyp-Trp(CHO)-NMeBzl

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / ethyl acetate / Ambient temperature

2: HOBT, WSCD / CH₂Cl₂ / Ambient temperature

3: HCl / CH₂Cl₂; ethyl acetate / Ambient temperature

4: HOBT, WSCD / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; benzotriazol-1-ol; In dichloromethane; ethyl acetate;
DOI:10.1021/jm00039a022