1,2-Hydrazinedicarboxylic acid, 1-(2,4,6-trimethoxyphenyl)-, 2-(2,2,2-trichloroethyl) 1-[2-(trimethylsilyl)ethyl] ester

Base Information

Chemical Name:1,2-Hydrazinedicarboxylic acid, 1-(2,4,6-trimethoxyphenyl)-, 2-(2,2,2-trichloroethyl) 1-[2-(trimethylsilyl)ethyl] ester
CAS No.:154876-23-0
Molecular Formula:C18H27Cl3N2O7Si
Molecular Weight:517.866
Hs Code.:
Mol file:154876-23-0.mol

Synonyms:

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Chemical Property of 1,2-Hydrazinedicarboxylic acid, 1-(2,4,6-trimethoxyphenyl)-, 2-(2,2,2-trichloroethyl) 1-[2-(trimethylsilyl)ethyl] ester

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Technology Process of 1,2-Hydrazinedicarboxylic acid, 1-(2,4,6-trimethoxyphenyl)-, 2-(2,2,2-trichloroethyl) 1-[2-(trimethylsilyl)ethyl] ester

There total 5 articles about 1,2-Hydrazinedicarboxylic acid, 1-(2,4,6-trimethoxyphenyl)-, 2-(2,2,2-trichloroethyl) 1-[2-(trimethylsilyl)ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 621-23-8
1,2,3-trimethoxybenzene

: 2-(trimethylsilyl)ethyl 2,2,2-trichloroethyl azodicarboxylate

: 154876-23-0
1-(2,4,6-trimethoxyphenyl)-1,2-hydrazinedicarboxylic acid 1-<2-(trimethylsilyl)ethyl> 2-(2,2,2-trichloroethyl) ester

Guidance literature:: With zinc(II) iodide; In diethyl ether; dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jo00082a035

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 154876-23-0
1-(2,4,6-trimethoxyphenyl)-1,2-hydrazinedicarboxylic acid 1-<2-(trimethylsilyl)ethyl> 2-(2,2,2-trichloroethyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: 54 percent / pyridine / CHCl₃ / 18 h / Heating

2: 97 percent / aq. NH₂NH₂ / Heating

3: 87 percent / CH₂Cl₂ / 8 h / Ambient temperature

4: 78 percent / N₂O₄ / CH₂Cl₂ / Ambient temperature

5: 83 percent / ZnI₂ / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With pyridine; dinitrogen tetraoxide; hydrazine hydrate; zinc(II) iodide; In diethyl ether; dichloromethane; chloroform;
DOI:10.1021/jo00082a035

Reference yield:

: 154876-20-7
1-hydrazinecarboxylic acid 2-(trimethylsilyl)ethyl ester

: 154876-23-0
1-(2,4,6-trimethoxyphenyl)-1,2-hydrazinedicarboxylic acid 1-<2-(trimethylsilyl)ethyl> 2-(2,2,2-trichloroethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / CH₂Cl₂ / 8 h / Ambient temperature

2: 78 percent / N₂O₄ / CH₂Cl₂ / Ambient temperature

3: 83 percent / ZnI₂ / CH₂Cl₂; diethyl ether / 3 h / Ambient temperature

With dinitrogen tetraoxide; zinc(II) iodide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00082a035