5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

Base Information

Chemical Name:5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one
CAS No.:22743-05-1
Molecular Formula:C₂₀H₁₂O₇
Molecular Weight:364.311
Hs Code.:
Mol file:22743-05-1.mol

Synonyms:Furo[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one,9-hydroxy-5-[3,4-(methylenedioxy)phenyl]- (8CI); Taiwanin E

Suppliers and Price of 5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of 5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

Chemical Property:

PSA：83.45000
LogP:3.34020

Purity/Quality:: 97.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

There total 34 articles about 5-(1,3-Benzodioxol-5-yl)-9-hydroxyfuro[3',4':6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 136003-82-2
(5aα,8aα,9α)-9-(1,3-benzodioxol-5-yl)-5a,6,8a,9-tetrahydro-9-hydroxyfuro<3',4':6,7>naphtho<2,3-d>-1,3-dioxole-5,8-dione

: 22743-05-1
5-(1,3-benzodioxol-5-yl)-9-hydroxyfuro[3′,4′:6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 16h; Heating;
DOI:10.1016/S0040-4020(01)91221-9

Reference yield: 89.0%

: potassium (3,4-(methylenedioxy)phenyl)trifluoroborate

: 1621253-42-6
9-[(tert-butoxycarbonyl)oxy]-6-oxo-6,8-dihydrofuro[3′,4′:6,7]-naphtho[2,3-d][1,3]dioxol-5-yl trifluoromethanesulfonate

: 22743-05-1
5-(1,3-benzodioxol-5-yl)-9-hydroxyfuro[3′,4′:6,7]naphtho[2,3-d]-1,3-dioxol-6(8H)-one

Guidance literature:: With palladium diacetate; caesium carbonate; tricyclohexylphosphine; In 1,4-dioxane; water; at 120 ℃; for 17h;
DOI:10.1002/ejoc.201601611