1H-Pyrrole-3-carboxylic acid, 1-(methoxymethyl)-5-[1-[(4-methylphenyl)sulfonyl]-2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-, methyl ester

Base Information

Chemical Name:1H-Pyrrole-3-carboxylic acid, 1-(methoxymethyl)-5-[1-[(4-methylphenyl)sulfonyl]-2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-, methyl ester
CAS No.:155474-10-5
Molecular Formula:C26H29NO9S
Molecular Weight:531.584
Hs Code.:
Mol file:155474-10-5.mol

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Chemical Property of 1H-Pyrrole-3-carboxylic acid, 1-(methoxymethyl)-5-[1-[(4-methylphenyl)sulfonyl]-2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-, methyl ester

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Technology Process of 1H-Pyrrole-3-carboxylic acid, 1-(methoxymethyl)-5-[1-[(4-methylphenyl)sulfonyl]-2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-, methyl ester

There total 4 articles about 1H-Pyrrole-3-carboxylic acid, 1-(methoxymethyl)-5-[1-[(4-methylphenyl)sulfonyl]-2-oxo-2-(3,4,5-trimeth oxyphenyl)ethyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 647864-38-8
methyl 2-[2-hydroxy-2-(3,4,5-trimethoxyphenyl)-1-tosylethyl]-N-methoxymethylpyrrole-4-carboxylate

: 155474-10-5
methyl N-methoxymethyl-2-[2-oxo-2-(3,4,5-trimethoxyphenyl)-1-tosylethyl]pyrrole-4-carboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chlorobenzene; for 4.5h; Heating;
DOI:10.1021/ol0357954

Reference yield: 62.0%

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 647864-38-8
methyl 2-[2-hydroxy-2-(3,4,5-trimethoxyphenyl)-1-tosylethyl]-N-methoxymethylpyrrole-4-carboxylate

: 155474-10-5
methyl N-methoxymethyl-2-[2-oxo-2-(3,4,5-trimethoxyphenyl)-1-tosylethyl]pyrrole-4-carboxylate

Guidance literature:: In dichloromethane; toluene;

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 155474-10-5
methyl N-methoxymethyl-2-[2-oxo-2-(3,4,5-trimethoxyphenyl)-1-tosylethyl]pyrrole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropylamide / tetrahydrofuran; hexane / 0.58 h / -78 - -60 °C

1.2: 88 percent / hexane; tetrahydrofuran / 1 h / -50 °C

2.1: 100 percent / DDQ / chlorobenzene / 4.5 h / Heating

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; hexane; chlorobenzene;
DOI:10.1021/ol0357954