3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester

Base Information

• Chemical Name: 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester
• CAS No.: 29579-95-1
• Molecular Formula: C₁₆H₂₆O₂
• Molecular Weight: 250.381
• Mol file: 29579-95-1.mol

Synonyms:

Chemical Property of 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester

There total 2 articles about 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + diethoxyphosphoryl-acetic acid ethyl ester (867-13-0) + 4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on (17283-81-7) → 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester (29579-95-1)

Guidance literature:

Multistep reaction;

DOI:10.1016/S0040-4020(01)93072-8

Reference yield:

→ 3-Methylen-5-(2,6,6-trimethyl-cyclohexenyl(1)>-valeriansaeuremethylester (29579-95-1)

Guidance literature:

aus Dihydro-β-ionon u. Triethylphosphonoacetat, dann CH2N2;

DOI:10.1039/C19670001257

upstream raw materials:

diazomethane

diethoxyphosphoryl-acetic acid ethyl ester

4-(2,6,6-Trimethyl-cyclohex-1-enyl)-butan-2-on