Technology Process of Benzothiazole, 2-(cyclopentylthio)-
There total 1 articles about Benzothiazole, 2-(cyclopentylthio)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydridotetakis(triphenylphosphine)rhodium(I); o-phenylenebis(diphenylphosphine);
In
chlorobenzene;
for 6h;
Inert atmosphere;
Reflux;
DOI:10.3987/COM-19-14147
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / water; ethanol / 75 h / 20 °C / Inert atmosphere
2: N-Bromosuccinimide; lithium hexamethyldisilazane / tetrahydrofuran / 5 h / 0 °C / Inert atmosphere; Schlenk technique
3: potassium carbonate; fac-tris(2-phenylpyridinato-N,C2')iridium(III); tert-dodecanethiol / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere; Irradiation
With
N-Bromosuccinimide; fac-tris(2-phenylpyridinato-N,C2')iridium(III); hexaammonium heptamolybdate tetrahydrate; tert-dodecanethiol; dihydrogen peroxide; potassium carbonate; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.201915837
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide; ammonium molybdate tetrahydrate / water; ethanol / 75 h / 20 °C / Inert atmosphere
2: lithium hexamethyldisilazane; N-Bromosuccinimide / tetrahydrofuran / 5 h / 0 °C / Schlenk technique; Inert atmosphere
3: fac-tris(2-phenylpyridinato-N,C2')iridium(III); potassium chloride / N,N-dimethyl-formamide / 13 h / 20 °C / Inert atmosphere; Irradiation
With
N-Bromosuccinimide; fac-tris(2-phenylpyridinato-N,C2')iridium(III); ammonium molybdate tetrahydrate; potassium chloride; dihydrogen peroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.202000088
