1,8(2H,5H)-Acridinedione, 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)-

Base Information

• Chemical Name: 1,8(2H,5H)-Acridinedione, 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)-
• CAS No.: 156176-94-2
• Molecular Formula: C23H26N2O4
• Molecular Weight: 394.47
• Mol file: 156176-94-2.mol

Synonyms:3,3,6,6-tetramethyl-9-(3-nitrophenyl)-3,4,6,7,9,10-hexahydro-(2H,5H)-acridine-1,8-dione;3,3,6,6-tetramethyl-9-(3-nitrophenyl)-3,4,6,7,9,10-hexahydro-1,8-(2H,5H)-acridinedione;3,3,6,6-tetramethyl-9-(3-nitrophenyl)-1,8-dioxo-1,2,3,4,5,6,7,8,9,10-decahydroacridine;3,3,6,6-tetramethyl-9-(3-nitrophenyl)-3,4,6,7-tetrahydroacridine-1,8(2H,5H,9H,10H)-dione;3,3,6,6-Tetramethyl-9-(3-nitro-phenyl)-3,4,6,7,9,10-hexahydro-2H,5H-acridine-1,8-dione;3,4,6,7-tetrahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)acridine-1,8(2H,5H,9H,10H)-dione;3,3,6,6-tetramethyl-9-(3-nitrophenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridin-1,8-dione;

Chemical Property of 1,8(2H,5H)-Acridinedione, 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)-

Chemical Property:

• Melting Point: 284-285 °C
• Boiling Point: 559.3±50.0 °C(Predicted)
• PSA: 91.99000
• Density: 1.26±0.1 g/cm3(Predicted)
• LogP: 5.42000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,8(2H,5H)-Acridinedione, 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)-

There total 7 articles about 1,8(2H,5H)-Acridinedione, 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9-(3-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-nitro-benzaldehyde (99-61-6) + dimedone (126-81-8) → 3,3,6,6-tetramethyl-9-(3-nitrophenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione (156176-94-2)

Guidance literature:

With ammonium acetate; In water; at 20 ℃; for 0.183333h; chemoselective reaction; Ionic liquid;

Reference yield: 94.0%

3-Nitrobenzyl alcohol (619-25-0) + dimedone (126-81-8) → 3,3,6,6-tetramethyl-9-(3-nitrophenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione (156176-94-2)

Guidance literature:

With aluminum(III) hydrogen sulfate; ammonium acetate; sodium bromide; sodium nitrite; In neat (no solvent); at 20 ℃; for 0.5h; Green chemistry;

DOI:10.1134/S1070363216060281

Reference yield: 80.0%

3-nitrobenzaldoxime (3431-62-7,20747-39-1) + dimedone (126-81-8) → 3,3,6,6-tetramethyl-9-(3-nitrophenyl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione (156176-94-2)

Guidance literature:

With ammonium acetate; In ethylene glycol; for 0.1h; microwave irradiation;

DOI:10.1055/s-2003-44981

upstream raw materials:

3-nitro-benzaldehyde

dimedone

3-nitrobenzaldoxime

1-amino-5,5-dimethylcyclohexen-3-one