N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine

Base Information

Chemical Name:N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine
CAS No.:156424-67-8
Molecular Formula:C12H11ClN2O
Molecular Weight:234.68200
Hs Code.:
DSSTox Substance ID:DTXSID701226094
Mol file:156424-67-8.mol

Synonyms:Oprea1_428155;DTXSID701226094;156424-67-8

Suppliers and Price of N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(Z)-6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME 95.00%
5MG
$ 499.92

Total 1 raw suppliers

Chemical Property of N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine

Chemical Property:

Boiling Point:475.9±33.0 °C(Predicted)
PKA:12.30±0.20(Predicted)
PSA：48.38000
Density:1.50±0.1 g/cm3(Predicted)
LogP:3.33590
XLogP3:3.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:234.0559907
Heavy Atom Count:16
Complexity:307

Purity/Quality:: (Z)-6-CHLORO-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-ONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2=C(C(=NO)C1)NC3=C2C=C(C=C3)Cl

Technology Process of N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine

There total 2 articles about N-(6-chloro-2,3,4,9-tetrahydrocarbazol-1-ylidene)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14192-67-7
6-chloro-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 156424-67-8
6-chloro-1-hydroxyimino-1,2,3,4-tetrahydrocarbazole

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol;

Reference yield:

: 1093413-54-7
C₁₅H₁₂ClNO₄

: 156424-67-8
6-chloro-1-hydroxyimino-1,2,3,4-tetrahydrocarbazole

Guidance literature:: With potassium hydroxide; hydroxylamine hydrochloride; In ethanol;
DOI:10.3184/030823407X266324

Reference yield: 44.0%

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 156424-67-8
6-chloro-1-hydroxyimino-1,2,3,4-tetrahydrocarbazole

: 7-chloro-3-phenyl-10H-2-oxa-1,10-diaza-cyclopenta[a]fluorene

Guidance literature:: 6-chloro-1-hydroxyimino-1,2,3,4-tetrahydrocarbazole; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 1h;

benzoic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 0.5h;

With hydrogenchloride; water; In tetrahydrofuran; for 1h; Heating;
DOI:10.1515/znb-1999-0918