Bicyclo[4.2.2]deca-2,4,7,9-tetraene

Base Information Edit

Chemical Name:Bicyclo[4.2.2]deca-2,4,7,9-tetraene
CAS No.:15677-13-1
Molecular Formula:C₁₀H₁₀
Molecular Weight:130.189
Hs Code.:2902199090
DSSTox Substance ID:DTXSID50701277
Mol file:15677-13-1.mol

Synonyms:Bicyclo[4.2.2]deca-2,4,7,9-tetraene;15677-13-1;DTXSID50701277

Suppliers and Price of Bicyclo[4.2.2]deca-2,4,7,9-tetraene

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[4.2.2]deca-2,4,7,9-tetraene Edit

Chemical Property:

PSA：0.00000
LogP:2.47080
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:130.078250319
Heavy Atom Count:10
Complexity:190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2C=CC(C=C1)C=C2

Technology Process of Bicyclo[4.2.2]deca-2,4,7,9-tetraene

There total 18 articles about Bicyclo[4.2.2]deca-2,4,7,9-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75891-04-2
2,3-Diazatricyclo<5.3.2.0^4,10>dodeca-2,5,8,11-tetraen

: 15677-13-1
bicyclo<4.2.2>deca-2,4,6,9-tetraene

: 1005-51-2
Bullvalen

Guidance literature:: In chloroform-d1; for 1h; Product distribution; Rate constant; Heating; half-life time t1/2=31 min, further photolysis, other times and solvents;

Reference yield: 84.0%

: 477773-51-6
cyclooctatetraene

: 74-86-2,25067-58-7
acetylene

: 15677-13-1
Bicyclo<4.2.2>deca-2,4,7,9-tetraen

Guidance literature:: With cobalt(II) bromide-[1,2-bis(diphenylphosphino)ethane]; zinc(II) iodide; zinc; In 1,2-dichloro-ethane; for 4.5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201712157

Reference yield:

: 34733-74-9
bicyclo[4.2.1]nona-2,4,7-trien-9-one

: 15677-13-1
Bicyclo<4.2.2>deca-2,4,7,9-tetraen

Guidance literature:: Multi-step reaction with 4 steps

1: 4,4'-bis-dimethylamino-benzophenone / Irradiation

2: methanol

3: aq. HCl

4: MeLi

With hydrogenchloride; methyllithium; bis(p-dimethylaminophenyl)methanone; In methanol;
DOI:10.1021/jo00905a007