Ethanimidoyl chloride, N-(2,6-dimethylphenyl)-

Base Information

• Chemical Name: Ethanimidoyl chloride, N-(2,6-dimethylphenyl)-
• CAS No.: 157894-09-2
• Molecular Formula: C10H12ClN
• Molecular Weight: 181.665
• Mol file: 157894-09-2.mol

Synonyms:

Chemical Property of Ethanimidoyl chloride, N-(2,6-dimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethanimidoyl chloride, N-(2,6-dimethylphenyl)-

There total 2 articles about Ethanimidoyl chloride, N-(2,6-dimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dimethylaniline (87-62-7) → N-(2,6-dimethylphenyl)acetimidoyl chloride2 (157894-09-2)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: bis(trichloromethyl) carbonate

With bis(trichloromethyl) carbonate; In dichloromethane;

DOI:10.1021/acs.inorgchem.8b01656

Reference yield:

N-(2,6-dimethylphenyl)acetamide (2198-53-0) → N-(2,6-dimethylphenyl)acetimidoyl chloride2 (157894-09-2)

Guidance literature:

With phosphorus pentachloride; Heating; Neat (no solvent);

DOI:10.1039/c0dt00498g

Reference yield: 98.0%

2-methylimidazole (693-98-1) + N-(2,6-dimethylphenyl)acetimidoyl chloride2 (157894-09-2) → C14H18N3(1+)*Cl(1-) (1449134-20-6)

Guidance literature:

In tetrahydrofuran; for 20h; Inert atmosphere;

DOI:10.1021/om400268y

upstream raw materials:

N-(2,6-dimethylphenyl)acetamide

2,6-dimethylaniline

Downstream raw materials:

tributyl[1-(2,6-xylylimino)ethyl]stannane

3-[1-((2,6-dimethylphenyl)amino)ethylidene]-1,1,1,5,5,5-hexafluoropentane-2,4-dione

N-(1-(2,6-dimethylphenylimino)ethyl)-1,3-bis(2,6-diisopropylphenyl)imidazol-2-imine hydrochloride

N-(1-(2,6-dimethylphenylimino)ethyl)-1,3-bis(2,4,6-trimethylphenyl)imidazol-2-imine hydrochloride