N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine

Base Information

Chemical Name:N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine
CAS No.:157949-12-7
Molecular Formula:C14H19N
Molecular Weight:201.312
Hs Code.:
DSSTox Substance ID:DTXSID00571982
Wikidata:Q82460199
Mol file:157949-12-7.mol

Synonyms:157949-12-7;N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine;DTXSID00571982

Suppliers and Price of N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:201.151749610
Heavy Atom Count:15
Complexity:180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCN(CC=C)CC1=CC=CC=C1

Technology Process of N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine

There total 3 articles about N-Benzyl-N-(prop-2-en-1-yl)but-3-en-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 17150-62-8
N-benzyl-3-butenylamine

: 106-95-6
allyl bromide

: 157949-12-7
N-allyl-N-benzyl-N-(3-butenyl)amine

Guidance literature:: With potassium carbonate; In acetonitrile; for 48h; Ambient temperature;
DOI:10.1055/s-1998-5923

Reference yield: 53.0%

: N-benzyl-N-(3-butenyl)-N-(2-chloroallyl)amine

: N-benzyl-4-methyl-3-methylenepiperidine

: 160718-78-5
N-allyl-N-butylbenzylamine

: 157949-12-7
N-allyl-N-benzyl-N-(3-butenyl)amine

Guidance literature:: N-benzyl-N-(3-butenyl)-N-(2-chloroallyl)amine; With n-butyllithium; zirconocene dichloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With sodium hydrogencarbonate; In methanol; at 20 ℃; for 16h;
DOI:10.1055/s-2005-870029

Reference yield:

: 17150-62-8
N-benzyl-3-butenylamine

: 157949-12-7
N-allyl-N-benzyl-N-(3-butenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 58 percent / K₂CO₃ / acetonitrile / 19 h / Heating

2.1: ZrCp₂Cl₂; n-BuLi / tetrahydrofuran; hexane / -78 - 20 °C

2.2: aq. NaHCO₃ / methanol / 16 h / 20 °C

With n-butyllithium; zirconocene dichloride; potassium carbonate; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1055/s-2005-870029