Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester

Base Information

Chemical Name:Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester
CAS No.:15802-69-4
Molecular Formula:C13H13NO5
Molecular Weight:263.25
Hs Code.:
Mol file:15802-69-4.mol

Synonyms:2-(4-nitrobenzylidene)acetoacetic acid ethyl ester;2-Acetyl-3-(4-nitro-phenyl)-acrylsaeure-aethylester;Butanoic acid,2-[(4-nitrophenyl)methylene]-3-oxo-,ethyl ester;2-[(4-nitrophenyl)methylene]-3-oxobutanoic acid,ethyl ester;ethyl 2-(4-nitrobenzylidene)-3-oxobutanoate;2-acetyl-3-(4-nitro-phenyl)-acrylic acid ethyl ester;

Suppliers and Price of Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester

Chemical Property:

Melting Point:164 °C(Solv: ethanol (64-17-5))
Boiling Point:380.6±27.0 °C(Predicted)
PSA：89.19000
Density:1.261±0.06 g/cm3(Predicted)
LogP:2.65350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester

There total 14 articles about Butanoic acid, 2-[(4-nitrophenyl)methylene]-3-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 141-97-9
ethyl acetoacetate

: 555-16-8
4-nitrobenzaldehdye

: 15802-69-4
ethyl 2-(4-nitrobenzylidene)-3-oxobutanoate

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1007/s11164-011-0322-y

Reference yield: 75.0%

: 3-acetoxy-1-ethoxy-3-(p-nitrophenyl)-1-propyne

: 15802-69-4,52351-77-6,20047-97-6
2-(4-nitrophenylmethylene)acetoacetic acid ethyl ester

Guidance literature:: platinum(II) chloride; In dichloromethane; at 20 ℃;
DOI:10.1021/ja072864r

Reference yield: 74.0%

: 141-97-9
ethyl acetoacetate

: 555-16-8
4-nitrobenzaldehdye

: 15802-69-4,52351-77-6,20047-97-6
2-(4-nitrophenylmethylene)acetoacetic acid ethyl ester

Guidance literature:: With lipase lipoprotein from Aspergillus niger; In dimethyl sulfoxide; at 35 ℃; for 48h; Green chemistry; Enzymatic reaction;
DOI:10.1016/j.catcom.2015.02.007