Borate(1-), tetramethoxy-

Base Information

Chemical Name:Borate(1-), tetramethoxy-
CAS No.:15841-16-4
Molecular Formula:C₄H₁₂BO₄
Molecular Weight:134.948
Hs Code.:
Mol file:15841-16-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Borate(1-), tetramethoxy-

Chemical Property:

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Technology Process of Borate(1-), tetramethoxy-

There total 2 articles about Borate(1-), tetramethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: lithium pentafluorophenyltrimethoxyborate

: 912292-12-7
bis(pentafluorophenyl)dimethoxyborate anion

: 15841-16-4
tetrakis-(methanolato-O)-borate^(1-)

Guidance literature:: With catalyst: TMEDA; In dichloromethane; under Ar, teflon-perfluoropropylene block copolymer vessel, 32 °C, 10 min, 0.11, 0.21, 0.31, 0.48, 0.60 and 0.72, 0.84, 1.10, 1.20, 1.35,1.60 and 2.20 equiv. of TMEDA was added; trimethoxy:dimethoxy compd. molar ratio was determined by (19)F NMR, they have been 58:42, 36:64, 23:77, 16:84 and 11:89, resp., at the first 5 TMEDA amounts, and 2:98 at the other TMEDA amounts;
DOI:10.1002/zaac.200500083

Reference yield:

: lithium pentafluorophenyltrimethoxyborate

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: (N,N,N',N'-tetramethyl-1,2-ethylenediamine)lithium bis(pentafluorophenyl)dimethoxyborate

: 15841-16-4
tetrakis-(methanolato-O)-borate^(1-)

Guidance literature:: In dichloromethane; under Ar, perfluorinated ethene and perfluorinated propene block coplymer vessel, 1.3 equiv. of TMEDA was added to Li-compd. soln.; pentane was layered, storage at -78 °C for 3 weeks;
DOI:10.1002/zaac.200500083