Benzoic acid, 3,4,5-tris(decyloxy)-, methyl ester

Base Information

• Chemical Name: Benzoic acid, 3,4,5-tris(decyloxy)-, methyl ester
• CAS No.: 158921-39-2
• Molecular Formula: C38H68O5
• Molecular Weight: 604.955
• Mol file: 158921-39-2.mol

Synonyms:methyl 3,4,5-tris(decyloxy)benzoate;Benzoic acid,3,4,5-tris(decyloxy)-,methyl ester;methyl 3,4,5-tris(n-decan-1-yloxy)benzoate;methyl 3,4,5-tri-n-decyloxybenzoate;

Chemical Property of Benzoic acid, 3,4,5-tris(decyloxy)-, methyl ester

Chemical Property:

• PSA: 53.99000
• LogP: 12.03170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3,4,5-tris(decyloxy)-, methyl ester

There total 3 articles about Benzoic acid, 3,4,5-tris(decyloxy)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-bromo dodecane (112-29-8) + methyl galloate (99-24-1) → methyl 3,4,5-tris(n-decan-1-yloxy)benzoate (158921-39-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jacs.0c02398

Reference yield: 40.0%

1-bromo dodecane (112-29-8) + methyl galloate (99-24-1) → C28H48O5 + methyl 3,4,5-tris(n-decan-1-yloxy)benzoate (158921-39-2)

Guidance literature:

With potassium carbonate;

DOI:10.1039/c5ra05983f

Reference yield:

3,4,5-trihydroxybenzoic acid (149-91-7) → methyl 3,4,5-tris(n-decan-1-yloxy)benzoate (158921-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / methanol / Reflux

2: potassium carbonate / ethanol / 24 h / Reflux

With sulfuric acid; potassium carbonate; In methanol; ethanol; 2: |Williamson Ether Synthesis;

DOI:10.1080/15421406.2013.781489

upstream raw materials:

1-bromo dodecane

methyl galloate

3,4,5-trihydroxybenzoic acid

Downstream raw materials:

1,5-Bis-(3,4,5-tris-decyloxy-phenyl)-pentane-1,3,5-trione

ethyl 3,4,5-tris(decyloxy)benzhydrazide

3,4,5-tris(n-decan-1-yloxy)benzoyl chloride

3,4,5-tris(decyloxy)benzaldehyde