N-methylbenzenesulfonimidoyl chloride

Base Information

Chemical Name:N-methylbenzenesulfonimidoyl chloride
CAS No.:15934-21-1
Molecular Formula:C7H8ClNOS
Molecular Weight:189.66300
Hs Code.:
DSSTox Substance ID:DTXSID40500332
Mol file:15934-21-1.mol

Synonyms:N-methylbenzenesulfonimidoyl chloride;15934-21-1;DTXSID40500332;(S-chloro-N-methylsulfonimidoyl)benzene

Suppliers and Price of N-methylbenzenesulfonimidoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-methylbenzenesulfonimidoyl chloride

Chemical Property:

PSA：37.81000
LogP:3.16280
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:189.0015127
Heavy Atom Count:11
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN=S(=O)(C1=CC=CC=C1)Cl

Technology Process of N-methylbenzenesulfonimidoyl chloride

There total 3 articles about N-methylbenzenesulfonimidoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69726-27-8
N-methyl-S-phenylsulfinamide

: 15934-21-1
N-methyl-S-phenylsulfonimidoyl chloride

Guidance literature:: With chlorine;
DOI:10.1021/jo01327a001

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 15934-21-1
N-methyl-S-phenylsulfonimidoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 20 °C

2.1: tert-butylhypochlorite / acetonitrile / 1 h / 20 °C

With oxalyl dichloride; tert-butylhypochlorite; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c7ob02028g