Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅)⁽¹⁺⁾*BF₄^(1-)=(Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅))BF₄

Base Information

• Chemical Name: Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅)⁽¹⁺⁾*BF₄^(1-)=(Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅))BF₄
• CAS No.: 99654-23-6
• Molecular Formula: BF₄*C₂₄H₂₆PPdS
• Molecular Weight: 570.735
• Mol file: 99654-23-6.mol

Synonyms:

Chemical Property of Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅)⁽¹⁺⁾*BF₄^(1-)=(Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅))BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅)⁽¹⁺⁾*BF₄^(1-)=(Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅))BF₄

There total 1 articles about Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅)⁽¹⁺⁾*BF₄^(1-)=(Pd(CH₂C(CH₃)CH₂)((C₆H₅)2PCH₂CH₂SC₆H₅))BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium tetrafluoroborate (13755-29-8) + (2-methylallyl)palladium-chloride dimer + (2-(phenylthio)ethyl)diphenylphosphine (19297-97-3) → Pd(CH2C(CH3)CH2)((C6H5)2PCH2CH2SC6H5)(1+)*BF4(1-)=(Pd(CH2C(CH3)CH2)((C6H5)2PCH2CH2SC6H5))BF4 (99654-23-6)

Guidance literature:

In methanol; a soln. of stoich. amt. of the ligand in MeOH was added dropwise to a stirred suspn. of Pd-complex in MeOH, 1 equiv. of NaBF4 was then added; soln. was evapd. to dryness in vacuo, residue recrystd. from CH2Cl2/i-PrOH, washed with Et2O; elem. anal.;

DOI:10.1016/0022-328X(85)87264-8

upstream raw materials:

sodium tetrafluoroborate

(2-(phenylthio)ethyl)diphenylphosphine