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Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate

Base Information Edit
  • Chemical Name:Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate
  • CAS No.:159635-22-0
  • Molecular Formula:C11H19NO3
  • Molecular Weight:213.27300
  • Hs Code.:2933399090
  • European Community (EC) Number:846-815-2
  • DSSTox Substance ID:DTXSID70442094
  • Nikkaji Number:J1.517.326B
  • Mol file:159635-22-0.mol
Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate

Synonyms:159635-22-0;TERT-BUTYL 3-HYDROXY-4-METHYLENEPIPERIDINE-1-CARBOXYLATE;1-Boc-3-Hydroxy-4-methylenepiperidine;tert-butyl 3-hydroxy-4-methylidenepiperidine-1-carboxylate;TERT-BUTYL-3-HYDROXY-4-METHYLENEIPERIDINE-1-CARBOXYLATE;N-Boc-3-hydroxy-4-methylenepiperidine;MFCD15474939;SCHEMBL733742;DTXSID70442094;1-Boc-4-methylene-3-piperidinol;IMRNHROGUGVTAI-UHFFFAOYSA-N;AMY35520;TERT-BUTYL 3-HYDROXY-4-METHYLENEIPERIDINE-1-CARBOXYLATE;AKOS015920024;PB13654;DS-13126;SY030116;CS-0048283;FT-0718275;EN300-317423;N-t-BOC-4-Methylene-3-Piperidinol, AldrichCPR;A883293;TERT-BUTYL3-HYDROXY-4-METHYLENEPIPERIDINE-1-CARBOXYLATE;3-hydroxy-4-methylene-piperidine-1-carboxylic acid tert-butyl ester;3-Hydroxy-4-methylenepiperidine-1-carboxylic acid tert-butyl ester;1-[(1,1-dimethylethoxy)carbonyl]-3-hydroxy-4-methylene-1,2,5,6-tetrahydropyridine;1-PIPERIDINECARBOXYLIC ACID, 3-HYDROXY-4-METHYLENE-, 1,1-DIMETHYLETHYL ESTER

Suppliers and Price of Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • Usbiological
  • 1-Boc-3-hydroxy-4-methylenepiperidine
  • 25mg
  • $ 319.00
  • TRC
  • 1-Boc-3-hydroxy-4-methylenepiperidine
  • 25mg
  • $ 55.00
  • TRC
  • 1-Boc-3-hydroxy-4-methylenepiperidine
  • 50mg
  • $ 95.00
  • Synthonix
  • 1-Boc-3-hydroxy-4-methylenepiperidine 95+%
  • 50g
  • $ 2740.00
  • SynQuest Laboratories
  • N-Boc-4-methylene-3-piperidinol
  • 250 mg
  • $ 175.00
  • SynQuest Laboratories
  • N-Boc-4-methylene-3-piperidinol
  • 1 g
  • $ 525.00
  • Matrix Scientific
  • 1-Boc-3-Hydroxy-4-methylenepiperidine 95+%
  • 1g
  • $ 958.00
  • Matrix Scientific
  • 1-Boc-3-Hydroxy-4-methylenepiperidine 95+%
  • 250mg
  • $ 445.00
  • J&W Pharmlab
  • tert-Butyl3-hydroxy-4-methyleneiperidine-1-carboxylate 98%
  • 1g
  • $ 115.00
  • Crysdot
  • tert-Butyl3-hydroxy-4-methylenepiperidine-1-carboxylate 95+%
  • 25g
  • $ 1027.00
Total 31 raw suppliers
Chemical Property of Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate Edit
Chemical Property:
  • Vapor Pressure:0mmHg at 25°C 
  • Boiling Point:309.018oC at 760 mmHg 
  • PKA:14.29±0.20(Predicted) 
  • Flash Point:140.689oC 
  • PSA:49.77000 
  • Density:1.092g/cm3 
  • LogP:1.48220 
  • Storage Temp.:2-8°C 
  • XLogP3:0.8
  • Hydrogen Bond Donor Count:1
  • Hydrogen Bond Acceptor Count:3
  • Rotatable Bond Count:2
  • Exact Mass:213.13649347
  • Heavy Atom Count:15
  • Complexity:268
Purity/Quality:

98%,99%, *data from raw suppliers

1-Boc-3-hydroxy-4-methylenepiperidine *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
  • Canonical SMILES:CC(C)(C)OC(=O)N1CCC(=C)C(C1)O
Technology Process of Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate

There total 5 articles about Tert-butyl 3-hydroxy-4-methylenepiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
4-benzenesulfinylmethyl-4-hydroxy-piperidine-1-carboxylic acid tert-butyl ester; With potassium tert-butylate; In tert-butyl alcohol; for 2h; Reflux; Inert atmosphere;
With ammonium chloride; In tert-butyl alcohol; for 0.166667h;
Guidance literature:
With tert.-butylhydroperoxide; selenium(IV) oxide; In decane; dichloromethane; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/jo0007682
Guidance literature:
With diisopropylamine; In tetrahydrofuran; N,N',N''-triethylenephosphoramide; hexane; ethyl acetate; tert-butyl alcohol;
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