di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate

Base Information

• Chemical Name: di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate
• CAS No.: 96657-55-5
• Molecular Formula: C₄₄H₄₁ClN₂O₉
• Molecular Weight: 777.271

Synonyms:

Chemical Property of di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate

There total 3 articles about di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + (3S*,6S*)-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid (96657-51-1) → dimethyl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-53-3) + benzhydryl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>-6-methoxycarbonylperhydro-1,2-oxazine-3-carboxylate (96657-63-5) + methyl (3S*,6S*)-6-benzhydryl-oxycarbonyl-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3-carboxylate (96657-62-4) + di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-55-5)

Guidance literature:

With diazodiphenylmethane; Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, EtOH; 2.) Et₂O;

DOI:10.1016/S0040-4020(01)88799-8

Reference yield:

(3S*,6S*)-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid (96657-51-1) + diazodiphenylmethane (908093-98-1) → dimethyl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-53-3) + benzhydryl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>-6-methoxycarbonylperhydro-1,2-oxazine-3-carboxylate (96657-63-5) + methyl (3S*,6S*)-6-benzhydryl-oxycarbonyl-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3-carboxylate (96657-62-4) + di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-55-5)

Guidance literature:

With diazomethane; Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, EtOH; 2.) Et₂O;

DOI:10.1016/S0040-4020(01)88799-8

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + (3S*,6S*)-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid (96657-51-1) + diazodiphenylmethane (908093-98-1) → dimethyl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-53-3) + benzhydryl (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>-6-methoxycarbonylperhydro-1,2-oxazine-3-carboxylate (96657-63-5) + methyl (3S*,6S*)-6-benzhydryl-oxycarbonyl-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3-carboxylate (96657-62-4) + di(benzhydryl) (3S*,6S*)-2-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylate (96657-55-5)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) toluene, EtOH; 2.) Et₂O;

DOI:10.1016/S0040-4020(01)88799-8

upstream raw materials:

diazomethane

(3S*,6S*)-benzyloxycarbonyl-6-<methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

diazodiphenylmethane

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