6-FLUOROFLAVONE

Base Information

• Chemical Name: 6-FLUOROFLAVONE
• CAS No.: 1218-82-2
• Molecular Formula: C15H9 F O2
• Molecular Weight: 240.234
• Hs Code.: 2914700090
• Mol file: 1218-82-2.mol

Synonyms:Flavone,6-fluoro- (7CI,8CI); 6-Fluoroflavone; NSC 93394

Chemical Property of 6-FLUOROFLAVONE

Chemical Property:

• Vapor Pressure: 7.56E-06mmHg at 25°C
• Boiling Point: 375.8°Cat760mmHg
• Flash Point: 174.9°C
• PSA: 30.21000
• Density: 1.309g/cm³
• LogP: 3.59910

Purity/Quality:

99% ^*data from raw suppliers

6-Fluoroflavone ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-FLUOROFLAVONE

There total 24 articles about 6-FLUOROFLAVONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

6-fluoro-4H-chromen-4-one (105300-38-7) + phenylboronic acid (98-80-6) → 6-fluoro-2-phenylchromen-4-one (1218-82-2)

Guidance literature:

6-fluoro-4H-chromen-4-one; phenylboronic acid; With iron(III) trifluoromethanesulfonate; palladium diacetate; Trimethylacetic acid; at 60 ℃; under air;

With potassium nitrite; 2,3-dicyano-5,6-dichloro-p-benzoquinone;

DOI:10.1039/c2ob26061a

Reference yield: 96.0%

1-(5-fluoro-2-methoxyphenyl)-3-phenylpropane-1,3-dione → 6-fluoro-2-phenylchromen-4-one (1218-82-2)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 160 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

DOI:10.1002/adsc.202001169

Reference yield: 95.0%

1-(5-fluoro-2-hydroxyphenyl)-3-phenylpropane-1,3-dione (58483-26-4) → 6-fluoro-2-phenylchromen-4-one (1218-82-2)

Guidance literature:

With malic acid; In neat (no solvent); at 140 ℃; for 0.0833333h; Microwave irradiation; Green chemistry;

DOI:10.2174/157017861108140613163214

upstream raw materials:

1-(5-fluoro-2-hydroxyphenyl)-3-phenylpropane-1,3-dione

1-(5-fluoro-2-hydroxyphenyl)ethan-1-one

benzoyl chloride

benzaldehyde

Downstream raw materials:

C₂₁H₁₃FN₄O₅

6-fluoro-4-thioflavone

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