Stannane, [2,2'-bithiophen]-5-yltributyl-

Base Information

• Chemical Name: Stannane, [2,2'-bithiophen]-5-yltributyl-
• CAS No.: 162717-58-0
• Molecular Formula: C20H32S2Sn
• Molecular Weight: 455.316
• DSSTox Substance ID: DTXSID00458582
• Mol file: 162717-58-0.mol

Synonyms:Stannane, [2,2'-bithiophen]-5-yltributyl-;162717-58-0;[2,2'-bithiophen]-5-yltributylstannane;SCHEMBL1145183;DTXSID00458582;VXBHLQIFGXDFDS-UHFFFAOYSA-N;5-tributylstannyl-2,2'-bithiophene;5-(tributylstannyl)-2,2-bithiophene;2,2'-bithiophenyl-5-yltributylstannane;5-tri-n-butylstannyl-2,2'-bithiophene

Chemical Property of Stannane, [2,2'-bithiophen]-5-yltributyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 11
• Exact Mass: 456.096746
• Heavy Atom Count: 23
• Complexity: 299

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Sn](CCCC)(CCCC)C1=CC=C(S1)C2=CC=CS2

Technology Process of Stannane, [2,2'-bithiophen]-5-yltributyl-

There total 1 articles about Stannane, [2,2'-bithiophen]-5-yltributyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoanthracene-9,10-dione (572-83-8) + aluminum tri-sec-butoxide (2269-22-9) → 2-(tri-n-butyl)stannyl-5,2'-bithiophene (162717-58-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; cyclohexanol;

Reference yield: 90.0%

1,4-diiodo-2,3,5,6-tetramethylbenzene (3268-21-1) + 2-(tri-n-butyl)stannyl-5,2'-bithiophene (162717-58-0) → C26H22S4

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 130 ℃; for 16h; Inert atmosphere;

Reference yield: 89.0%

2-(tri-n-butyl)stannyl-5,2'-bithiophene (162717-58-0) + C86H96N2O2*C38H32I2N2O6 → C86H96N2O2*C54H42N2O6S4

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In various solvent(s); at 100 ℃;

DOI:10.1021/ja042535o

upstream raw materials:

2-bromoanthracene-9,10-dione

aluminum tri-sec-butoxide

Downstream raw materials:

3,6-dibutoxy-4,5-bis([2,2'-bithiophene]-5-yl)phthalonitrile

(2,5-bis-[2,2']bithiophenyl-5-yl-4-ethoxycarbonylmethoxy-phenoxy)-acetic acid ethyl ester

(C₆H₂(OCH₃)(C₄H₂SC₄H₃S))2BC₆H₂(CH₃CHCH₃)3

N1-(3-([2,2’-bithiophen]-5-yl)-6,7-dichloroquinoxalin-2-yl)-N4,N4-diethylbutane-1,4-diamine