Anthracene-2-carbonyl chloride

Base Information

Chemical Name:Anthracene-2-carbonyl chloride
CAS No.:16331-51-4
Molecular Formula:C15H9ClO
Molecular Weight:240.689
Hs Code.:
DSSTox Substance ID:DTXSID50579130
Wikidata:Q82469545

Synonyms:ANTHRACENE-2-CARBONYL CHLORIDE;16331-51-4;SCHEMBL8156791;DTXSID50579130

Suppliers and Price of Anthracene-2-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of Anthracene-2-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:4.37200
XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:240.0341926
Heavy Atom Count:17
Complexity:301

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C3C=C(C=CC3=CC2=C1)C(=O)Cl

Technology Process of Anthracene-2-carbonyl chloride

There total 1 articles about Anthracene-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84-54-8
2-methylanthracene-9,10-dione

: 16331-51-4
Anthracene-2-carboxylic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium dichromate; sulfuric acid

2: zinc dust; diluted ammonia

3: PCl₅

With potassium dichromate; ammonium hydroxide; phosphorus pentachloride; sulfuric acid; zinc;

Reference yield:

: 16331-51-4
Anthracene-2-carboxylic acid chloride

: 613-12-7
2-methylanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: 3,4-thiene-2,3-diylbis(dicyclohexylphosphine); nickel(II) acetylacetonate dihydrate / 1,4-dioxane; hexane / 16 h / 170 °C / Inert atmosphere; Sealed tube

With dmap; nickel(II) acetylacetonate dihydrate; 3,4-thiene-2,3-diylbis(dicyclohexylphosphine); triethylamine; In 1,4-dioxane; hexane; dichloromethane;
DOI:10.1021/acs.orglett.8b01233