Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester

Base Information

Chemical Name:Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester
CAS No.:6622-95-3
Molecular Formula:C₁₁H₁₁NO₅
Molecular Weight:237.212
Hs Code.:2915390090
DSSTox Substance ID:DTXSID901235748
Mol file:6622-95-3.mol

Synonyms:CBMicro_025911;Oprea1_799933;SCHEMBL5929271;DTXSID901235748;AKOS024331686;Phenol, 2-methoxy-4-(2-nitroethenyl)-, 1-acetate;ACETIC ACID 2-METHOXY-4-(2-NITRO-VINYL)-PHENYL ESTER

Suppliers and Price of Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester

Chemical Property:

Vapor Pressure:4.55E-05mmHg at 25°C
Boiling Point:349.9°C at 760 mmHg
Flash Point:153.1°C
PSA：81.35000
Density:1.259g/cm³
LogP:2.39110
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:237.06372245
Heavy Atom Count:17
Complexity:310

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=C(C=C(C=C1)C=C[N+](=O)[O-])OC

Technology Process of Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester

There total 4 articles about Acetic acid 2-methoxy-4-(2-nitro-vinyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-52-5
nitromethane

: 881-68-5
vanillin acetate

: 6622-95-3
4-acetoxy-3-methoxy-β-nitro-styrene

Guidance literature:: With ammonium acetate; for 14h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2020.113148

Reference yield:

: 104655-06-3
3-Methoxy-4-acetoxy-α-nitromethyl-benzylalkohol

: 6622-95-3
4-acetoxy-3-methoxy-β-nitro-styrene

Guidance literature:: With sodium acetate; In acetic anhydride;
DOI:10.1139/v61-141

Reference yield:

: 881-68-5
vanillin acetate

: 6622-95-3
4-acetoxy-3-methoxy-β-nitro-styrene

Guidance literature:: Multi-step reaction with 2 steps

1: (i) aq. NaOH, EtOH, (ii) aq. AcOH

2: NaOAc / acetic anhydride

With sodium acetate; In acetic anhydride;
DOI:10.1139/v61-141