[Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6

Base Information

Chemical Name:[Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6
CAS No.:929633-74-9
Molecular Formula:C₅₁H₄₃N₄OOsP₂*F₆P
Molecular Weight:1125.04
Hs Code.:

Synonyms:

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Chemical Property of [Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6

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Technology Process of [Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6

There total 1 articles about [Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium hexafluorophosphate

: 16971-31-6,36007-23-5
hydridocarbonylchlorotris(triphenylphosphine)osmium(II)

: 928201-97-2
1-methyl-2-(naphthyl-β-azo)-imidazole

: 929633-74-9
[Os(H)(CO)(PPh3)2(1-methyl-2-(naphthyl-β-azo)imidazole)]PF6

Guidance literature:: In tetrahydrofuran; soln. of org. compd. added to suspn. of Os compd., stirred and refluxed for 15 h under N2, cooled, filtered, filtrate concd. slowly in air, soln. of NH4PF6 added, kept in deep frezer overnight; filtered, washed with cold THF, dried in CaCl2 desiccator in vac., chromy. (silica gel, MeCN), evapd., dried over CaCl2 in vac.; elem. anal.;
DOI:10.1016/j.poly.2006.08.028