tetracarbonyl(1-phenylborinato)vanadium

Base Information

• Chemical Name: tetracarbonyl(1-phenylborinato)vanadium
• CAS No.: 90857-25-3
• Molecular Formula: C₁₅H₁₀BO₄V
• Molecular Weight: 315.995

Synonyms:

Chemical Property of tetracarbonyl(1-phenylborinato)vanadium

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Technology Process of tetracarbonyl(1-phenylborinato)vanadium

There total 1 articles about tetracarbonyl(1-phenylborinato)vanadium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Na(diglyme)2][V(CO)6] + sodium 1-phenylborinate (60552-40-1) + mercury dichloride → tetracarbonyl(1-phenylborinato)vanadium (90857-25-3)

Guidance literature:

In diethyl ether; under N2 in the dark, to Na(C5H5BPh) in ether added with stirring at room temp. HgCl2 in ether followed by dropwise addn. of V complex in ether, allowed to react for 1.5 h; filtered through sea sand, washed with 2.5% hydrochloric acid, filteredthrough Al2O3 (4% H2O), concd. in strong N2 stream up to satn., slowly cooled at -78°C; elem. anal.;

DOI:10.1016/0022-328X(84)80085-6

upstream raw materials:

sodium 1-phenylborinate

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