Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate

Base Information

Chemical Name:Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate
CAS No.:167545-91-7
Molecular Formula:C10H14N2O2
Molecular Weight:194.23000
Hs Code.:2933990090
Mol file:167545-91-7.mol

Synonyms:ethyl 4,5,6,7-tetrahydrobenzimidazole-5-carboxylate;4,5,6,7-tetrahydrobenzimidazole-5-carboxylic ethyl ester;4,5,6,7-Tetrahydro-1H-indazolcarbonsaeure;4,5,6,7-Tetrahydro-1H-benzoimidazole-5-carboxylic;4,5,6,7-tetrahydrobenzimidazole-5-carboxylic acid;4,5,6,7-tetrahydro-1H-1,3-benzodiazole-5-carboxylic acid;5-Carboxy-4,5,6,7-tetrahydrobenzimidazol;ethyl 4,5,6,7-tetrahydro-1H-benzimidazol-5-carboxylate;4,5,6,7-Tetrahydro-1H-benzimidazole-5-carboxylic acid;4,5,6,7-Tetrahydro-1h-benzoiMidazole-5-carboxylic acid,HCl;

Suppliers and Price of Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
4,5,6,7-tetrahydro-1H-Benzimidazole-6-carboxylicacidethylester 97.00%
25G
$ 4320.00

AccelPharmtech
4,5,6,7-tetrahydro-1H-Benzimidazole-6-carboxylicacidethylester 97.00%
5G
$ 2330.00

AccelPharmtech
4,5,6,7-tetrahydro-1H-Benzimidazole-6-carboxylicacidethylester 97.00%
1G
$ 2070.00

Total 3 raw suppliers

Chemical Property of Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate

Chemical Property:

Melting Point:145-150 °C
Boiling Point:386.0±30.0 °C(Predicted)
PKA:14.63±0.40(Predicted)
PSA：54.98000
Density:1.199±0.06 g/cm3(Predicted)
LogP:1.07770

Purity/Quality:

95% ^*data from raw suppliers

4,5,6,7-tetrahydro-1H-Benzimidazole-6-carboxylicacidethylester 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate

There total 2 articles about Ethyl 4,5,6,7-tetrahydro-1H-benzo[d]iMidazole-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 39086-05-0
ethyl 3-bromo-4-oxocyclohexanecarboxylate

: 77287-34-4,77287-35-5,60100-09-6
formamide

: 167545-91-7,167546-10-3
ethyl 4,5,6,7-tetrahydro-1H-benzimidazol-5-carboxylate

Guidance literature:: ethyl 3-bromo-4-oxocyclohexanecarboxylate; formamide; at 150 ℃; for 2h;

With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Further stages;
DOI:10.1016/j.ejmech.2011.01.042