2-(Methylamino)benzenecarbothioamide

Base Information

• Chemical Name: 2-(Methylamino)benzenecarbothioamide
• CAS No.: 32600-73-0
• Molecular Formula: C8H10 N2 S
• Molecular Weight: 166.2434
• DSSTox Substance ID: DTXSID60404328
• NSC Number: 141659

Synonyms:NSC141659;32600-73-0;DTXSID60404328;AKOS000261147;NSC-141659

Chemical Property of 2-(Methylamino)benzenecarbothioamide

Chemical Property:

• Vapor Pressure: 0.000273mmHg at 25°C
• Boiling Point: 322.8°C at 760 mmHg
• Flash Point: 149°C
• Density: 1.227g/cm³
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 166.05646950
• Heavy Atom Count: 11
• Complexity: 147

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNC1=CC=CC=C1C(=S)N

Technology Process of 2-(Methylamino)benzenecarbothioamide

There total 2 articles about 2-(Methylamino)benzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.1%

1-methyl-2-mercapto-2-thioxo-2,3-dihydro-1H-2λ5-benzo[1,3,2]diazaphosphinine-4-thione pyridinium salt → 2-methylaminothiobenzamide (32600-73-0)

Guidance literature:

With hydrogenchloride; In toluene; Heating;

DOI:10.3390/60400323

Reference yield:

→ 2-methylaminothiobenzamide (32600-73-0)

Guidance literature:

14 (R = H, R3 = CH3, R4 = H), H2S;

Reference yield: 53.0%

4-methoxyphenylchloroformate (7693-41-6) + 2-methylaminothiobenzamide (32600-73-0) → 4-methoxyphenyl N-(2-thiocarbamoylphenyl)-N-(methyl)carbamate

Guidance literature:

In diethyl ether; at 0 ℃; for 1h;

DOI:10.1002/poc.999

Downstream raw materials:

N-methyl-N-(2-thiocarbamoyl-phenyl)-benzamide

4,N-dimethyl-N-(2-thiocarbamoyl-phenyl)-benzamide

4-chloro-N-methyl-N-(2-thiocarbamoyl-phenyl)-benzamide

4-methoxy-N-methyl-N-(2-thiocarbamoyl-phenyl)-benzamide

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