Carbamic acid, [1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl ester
CAS No.:168161-91-9
Molecular Formula:C₃₂H₄₁N₅O₅Si
Molecular Weight:603.794
Hs Code.:

Carbamic acid,
[1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth
oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl
ester

Synonyms:

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Chemical Property of Carbamic acid, [1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl ester

There total 4 articles about Carbamic acid, [1-(3,3-dimethyl-2-oxobutyl)-2,3-dihydro-2-oxo-5-[1-[[2-(trimethylsilyl)eth oxy]methyl]-1H-imidazol-2-yl]-1H-1,4-benzodiazepin-3-yl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124676-19-3
2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine

: 168161-91-9
{1-(3,3-Dimethyl-2-oxo-butyl)-2-oxo-5-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: WSC / 0 - 25 °C

2: NH₃ / methanol

3: 1.) NaH / 1) DMF

With ammonia; sodium hydride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol;
DOI:10.1016/0960-894X(95)00557-A

Reference yield:

: 168161-89-5
2-(2-Aminobenzoyl)-1-((2-(trimethylsilyl)ethoxy)methyl)imidazole

: 168161-91-9
{1-(3,3-Dimethyl-2-oxo-butyl)-2-oxo-5-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: WSC / 0 - 25 °C

2: NH₃ / methanol

3: 1.) NaH / 1) DMF

With ammonia; sodium hydride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol;
DOI:10.1016/0960-894X(95)00557-A

Reference yield:

: (Benzotriazol-1-yl-{2-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazole-2-carbonyl]-phenylcarbamoyl}-methyl)-carbamic acid benzyl ester

: 168161-91-9
{1-(3,3-Dimethyl-2-oxo-butyl)-2-oxo-5-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-imidazol-2-yl]-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl}-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NH₃ / methanol

2: 1.) NaH / 1) DMF

With ammonia; sodium hydride; In methanol;
DOI:10.1016/0960-894X(95)00557-A