1H-Imidazole-4-carboxylic acid, 2-[2-(1H-indol-3-yl)-1-[[(phenylmethoxy)carbonyl]amino]ethyl]-5-methyl-, ethyl ester, (R)-

Base Information

Chemical Name:1H-Imidazole-4-carboxylic acid, 2-[2-(1H-indol-3-yl)-1-[[(phenylmethoxy)carbonyl]amino]ethyl]-5-methyl-, ethyl ester, (R)-
CAS No.:168470-54-0
Molecular Formula:C25H26N4O4
Molecular Weight:446.506
Hs Code.:
Mol file:168470-54-0.mol

Synonyms:

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Chemical Property of 1H-Imidazole-4-carboxylic acid, 2-[2-(1H-indol-3-yl)-1-[[(phenylmethoxy)carbonyl]amino]ethyl]-5-methyl-, ethyl ester, (R)-

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Technology Process of 1H-Imidazole-4-carboxylic acid, 2-[2-(1H-indol-3-yl)-1-[[(phenylmethoxy)carbonyl]amino]ethyl]-5-methyl-, ethyl ester, (R)-

There total 4 articles about 1H-Imidazole-4-carboxylic acid, 2-[2-(1H-indol-3-yl)-1-[[(phenylmethoxy)carbonyl]amino]ethyl]-5-methyl-, ethyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 168470-53-9
2-[(R)-2-Benzyloxycarbonylamino-3-(1H-indol-3-yl)-propionylamino]-3-oxo-butyric acid ethyl ester

: 168470-54-0
2-[(R)-1-Benzyloxycarbonylamino-2-(1H-indol-3-yl)-ethyl]-5-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: With ammonium acetate; acetic acid; for 16h; Heating;
DOI:10.1021/jm950591h

Reference yield:

: 20207-16-3
ethyl 2-amino-3-oxobutanoate hydrochloride

: 168470-54-0
2-[(R)-1-Benzyloxycarbonylamino-2-(1H-indol-3-yl)-ethyl]-5-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide; tetrahydrofuran / 1 h / Ambient temperature

2: 73 percent / ammonium acetate, acetic acid / 16 h / Heating

With 4-methyl-morpholine; ammonium acetate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm950591h

Reference yield:

: 133641-28-8
C₂₄H₂₆N₂O₆

: 168470-54-0
2-[(R)-1-Benzyloxycarbonylamino-2-(1H-indol-3-yl)-ethyl]-5-methyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide; tetrahydrofuran / 1 h / Ambient temperature

2: 73 percent / ammonium acetate, acetic acid / 16 h / Heating

With 4-methyl-morpholine; ammonium acetate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm950591h