2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ⁵-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

Base Information

• Chemical Name: 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ⁵-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole
• CAS No.: 130719-02-7
• Molecular Formula: C₁₈H₃₀N₂O₄P₂S
• Molecular Weight: 432.461

Synonyms:

Chemical Property of 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ⁵-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

Chemical Property:

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Useful:

Technology Process of 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ⁵-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

There total 2 articles about 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ⁵-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

8-Phenyl-tetrahydro-8λ5-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole (57680-64-5) → 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ5-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ5-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole (130719-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: S₈

2: Ambient temperature

With sulfur;

Reference yield:

2-Phenyl-[1,3,6,2]dioxazaphosphocane 2-sulfide (106418-18-2) + 3,3,7,7-tetramethyl-2,8-dioxa-5-aza-1λ3-phosphabicyclo(3,3,0)octane (75194-94-4) → 2,2,6,6-Tetramethyl-8-(2-phenyl-2-thioxo-2λ5-[1,3,6,2]dioxazaphosphocan-6-yl)-tetrahydro-8λ5-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole (130719-01-6) + 2,2,6,6-Tetramethyl-8-[2-(2-phenyl-2-thioxo-2λ5-[1,3,2]oxazaphospholidin-3-yl)-ethoxy]-tetrahydro-8λ5-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole (130719-02-7)

Guidance literature:

Title compound not separated from byproducts; Ambient temperature;

upstream raw materials:

2-Phenyl-[1,3,6,2]dioxazaphosphocane 2-sulfide

3,3,7,7-tetramethyl-2,8-dioxa-5-aza-1λ³-phosphabicyclo(3,3,0)octane

8-Phenyl-tetrahydro-8λ⁵-[1,3,2]oxazaphospholo[2,3-b][1,3,2]oxazaphosphole

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