dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph₃P)2N

Base Information

• Chemical Name: dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph₃P)2N
• CAS No.: 887373-88-8
• Molecular Formula: C₂₈H₃₃Cl₂O₅Sn*C₃₆H₃₀NP₂
• Molecular Weight: 1177.77
• Mol file: 887373-88-8.mol

Synonyms:

Chemical Property of dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph₃P)2N

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph₃P)2N

There total 1 articles about dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph₃P)2N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(aqua)chloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane + tetrabutylammonium thiocyanate (3674-54-2) → chloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenyl(thiocyanato)stannane tetrabutylammonium + [2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylbis(thiocyanato)stannane tetrabutylammonium + dichloro[2-(6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxabenzocyclopentadec-2-yl)ethyl]diphenylstannane (Ph3P)2N (887373-88-8)

Guidance literature:

In dichloromethane-d2; Sn complex mixed with 4 equiv. of n-Bu42NSCN in CD2Cl2; not isolated, detected by NMR;

DOI:10.1002/ejic.200500191

upstream raw materials:

tetrabutylammonium thiocyanate