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Technology Process of (2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester

(2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester

Base Information
  • Chemical Name:(2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester
  • CAS No.:66260-79-5
  • Molecular Formula:C18H17Cl3N2O6S
  • Molecular Weight:495.768
  • Hs Code.:
(2Ξ,7<i>R</i>)-4-methyl-9-oxo-8<i>t</i>'-(2-phenoxy-acetylamino)-(4<i>c</i><i>H</i>,7<i>r</i>'<i>H</i>)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.0<sup>2,4</sup>]nonane-2<i>r</i>-carboxylic acid 2,2,2-trichloro-ethyl ester

Synonyms:

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Chemical Property of (2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester
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Technology Process of (2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester

There total 1 articles about (2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxoacetic acid 2,2,2-trichloro-ethyl ester
5317-23-7

oxoacetic acid 2,2,2-trichloro-ethyl ester

<i>N</i>-[(3<i>R</i>)-2-oxo-4<i>c</i>-(2-oxo-propylsulfanyl)-azetidin-3<i>r</i>-yl]-2-phenoxy-acetamide
66289-85-8

N-[(3R)-2-oxo-4c-(2-oxo-propylsulfanyl)-azetidin-3r-yl]-2-phenoxy-acetamide

(2Ξ,7<i>R</i>)-4-methyl-9-oxo-8<i>t</i>'-(2-phenoxy-acetylamino)-(4<i>c</i><i>H</i>,7<i>r</i>'<i>H</i>)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.0<sup>2,4</sup>]nonane-2<i>r</i>-carboxylic acid 2,2,2-trichloro-ethyl ester
66260-79-5

(2Ξ,7R)-4-methyl-9-oxo-8t'-(2-phenoxy-acetylamino)-(4cH,7r'H)-3-oxa-6-thia-1-aza-tricyclo[5.2.0.02,4]nonane-2r-carboxylic acid 2,2,2-trichloro-ethyl ester

Guidance literature:
Multistep reaction; (i) benzene, (ii) SOCl2, 2,6-dimethyl-pyridine, THF, (iii) KOtBu, tBuOH;
upstream raw materials:

oxoacetic acid 2,2,2-trichloro-ethyl ester

N-[(3R)-2-oxo-4c-(2-oxo-propylsulfanyl)-azetidin-3r-yl]-2-phenoxy-acetamide

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