Cyclopropanecarboxylic acid, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (1S,2S,3R)-

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (1S,2S,3R)-
CAS No.:171417-59-7
Molecular Formula:C26H36O4Si
Molecular Weight:440.655
Hs Code.:
Mol file:171417-59-7.mol

Cyclopropanecarboxylic acid,
2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-,
1,1-dimethylethyl ester, (1S,2S,3R)-

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Chemical Property of Cyclopropanecarboxylic acid, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (1S,2S,3R)-

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Technology Process of Cyclopropanecarboxylic acid, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (1S,2S,3R)-

There total 2 articles about Cyclopropanecarboxylic acid, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (1S,2S,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 392655-74-2
(1S,2R,3S)-tert-butyl 2-acetoxymethyl-3-tert-butyldiphenylsiloxymethylcyclopropanecarboxylate

: 171417-59-7
(1S,2S,3R)-tert-butyl 2-tert-butyldiphenylsiloxymethyl-3-hydroxymethylcyclopropanecarboxylate

Guidance literature:: With potassium carbonate; In methanol; water; at 20 ℃; for 1.5h;
DOI:10.1021/jo010728d

Reference yield:

: 392656-08-5
(1S,2R,3S)-2-Acetoxymethyl-3-(tert-butyl-diphenyl-silanyloxymethyl)-cyclopropanecarboxylic acid

: 171417-59-7
(1S,2S,3R)-tert-butyl 2-tert-butyldiphenylsiloxymethyl-3-hydroxymethylcyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 10 mg / boron trifluoride diethyl etherate / CH₂Cl₂; cyclohexane / 0.5 h / 20 °C

2: 85 percent / K₂CO₃ / methanol; H₂O / 1.5 h / 20 °C

With boron trifluoride diethyl etherate; potassium carbonate; In methanol; dichloromethane; cyclohexane; water;
DOI:10.1021/jo010728d