Benzonitrile, 3,3'-azoxybis-

Base Information

Chemical Name:Benzonitrile, 3,3'-azoxybis-
CAS No.:17197-24-9
Molecular Formula:C₁₄H₈N₄O
Molecular Weight:248.244
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzonitrile, 3,3'-azoxybis-

Chemical Property:

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Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzonitrile, 3,3'-azoxybis-

There total 4 articles about Benzonitrile, 3,3'-azoxybis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2237-30-1
m-cyanoaniline

: 17197-24-9,71298-00-5
1,2-bis(3-cyanophenyl)diazene oxide

Guidance literature:: With fluorosulfonyl fluoride; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; water; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2021.153457

Reference yield: 91.0%

: 2237-30-1
m-cyanoaniline

: 17197-24-9,71298-00-5
bis(3-cyanophenyl)diazene oxide

: 619-24-9
3-nitrobenzonitrile

Guidance literature:: With selenium(IV) oxide; dihydrogen peroxide; In methanol; water; at 20 ℃; for 24h;
DOI:10.1055/s-2008-1067088

Reference yield:

: 619-24-9
3-nitrobenzonitrile

: 17197-24-9,71298-00-5
1,2-bis(3-cyanophenyl)diazene oxide

: 2237-30-1
m-cyanoaniline

Guidance literature:: With glucose dehydrogenase; D-glucose; nicotinamide adenine dinucleotide phosphate; vanadia; Met-Asn-Glu-Val-Leu-Lys-Thr-Leu-Lys-Asp-His-Arg-Ser-Ile-Arg-Ser-Tyr-Thr-Asp-Glu-Pro-Val-Ser-Pro-Glu-Gln-Leu-Asp-Asp-Ile-Ile-Gln-Ala-Val-Gln-Ala-Ala-Pro-Asn-Ser-Ile-Asn-Gly-Gln-Gln-Val-Thr-Val-Ile-Thr-Val-Gln-Asp-Glu-Glu-Arg-Lys-Lys-Lys-Ile-Ala-Glu-Leu-Ala-Gly-Gly-Gln-Val-Trp-Ile-Glu-Gln-Ala-Pro-Val-Phe-Leu-Leu-Phe-Cys-Ala-Asp-Phe-Asn-Arg-Ala-Lys-Ile-Ala-Leu-Glu-Lys-Asn-Gly-Glu-Thr-Leu-Ala-Ile-Thr-Asp-Gly-Met-Glu-Ser-Val-Leu-Val-Gly-Ala-Val-Asp-Ala-Gly-Ile-Ala-Leu-Gly-Thr-Ala-Thr-Ala-Ala-Ala-Glu-Ser-Met-Gly-Leu-Gly-Thr-Val-Pro-Ile-Gly-Ala-Val-Arg-Gly-Arg-Ala-Glu-Glu-Leu-Ile-Lys-Leu-Leu-Asn-Ile-Pro-Glu-Tyr-Val-Phe-Pro-Val-Ala-Gly-Leu-Val-Val-Gly-His-Pro-Ala-Asp-Arg-Ser-Ala-Lys-Lys-Pro-Arg-Leu-Pro-Leu-Ile-Asp-Ala-Tyr-Asp-Glu-Glu-Ile-Ser-Glu-Tyr-Met-Thr-Lys-Arg-Thr-Asn-Gly-Gln-Glu-Thr-Arg-Asn-Trp-Ser-Gln-Gly-Ile-Ser-Ala-Tyr-Tyr-Asn-Lys-Val-Tyr-Tyr-Pro-His-Ile-Arg-Glu-Met-Leu-Glu-Lys-GIn-Gly-Phe-Lys-Leu-Glu; nicotinamide adenine dinucleotide; In aq. phosphate buffer; tert-butyl methyl ether; at 35 ℃; for 18h; Reagent/catalyst; Enzymatic reaction;