3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-

Base Information

Chemical Name:3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-
CAS No.:172607-26-0
Molecular Formula:C12H17NOS
Molecular Weight:223.339
Hs Code.:
DSSTox Substance ID:DTXSID20444048
Mol file:172607-26-0.mol

Synonyms:172607-26-0;3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-;DTXSID20444048

Suppliers and Price of 3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:223.10308534
Heavy Atom Count:15
Complexity:232

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)C(C)(CSC1=CC=CC=C1N)O

Technology Process of 3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl-

There total 1 articles about 3-Buten-2-ol, 1-[(2-aminophenyl)thio]-2,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 34485-82-0
2,3-dimethyl-3,4-epoxy-1-butene

: 137-07-5
2-amino-benzenethiol

: 172607-26-0
2-hydroxy-2-methyl-3-methyl-1-(2-aminophenylthio)-3-butene

Guidance literature:: With potassium hydroxide; In ethanol; at 50 ℃; for 2h;
DOI:10.1080/00397919508011449

Reference yield: 87.0%

: 172607-26-0
2-hydroxy-2-methyl-3-methyl-1-(2-aminophenylthio)-3-butene

: 203511-09-5
(3-propenyl-3-methyl)-2H-3,4-dihydro-1,4-benzothiazine

: 4-(aminophenylthio)-2-methylbutane-1,3-diene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 2.5h; Heating;
DOI:10.1080/00397919809458690

Reference yield:

: 172607-26-0
2-hydroxy-2-methyl-3-methyl-1-(2-aminophenylthio)-3-butene

: C₁₂H₁₇N₃OS₂

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / H₂O / 2 h

2: hydrazine hydrate / ethanol; H₂O / 6 h / 20 °C

With hydrogenchloride; hydrazine hydrate; In ethanol; water; 1: Acylation / 2: Addition;