5-exo-phenylcyclohexenyltricarbonylmanganese

Base Information

• Chemical Name: 5-exo-phenylcyclohexenyltricarbonylmanganese
• CAS No.: 131414-33-0
• Molecular Formula: C₁₅H₁₃MnO₃
• Molecular Weight: 296.204
• Mol file: 131414-33-0.mol

Synonyms:

Chemical Property of 5-exo-phenylcyclohexenyltricarbonylmanganese

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of 5-exo-phenylcyclohexenyltricarbonylmanganese

There total 1 articles about 5-exo-phenylcyclohexenyltricarbonylmanganese which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium aluminium tetrahydride (16853-85-3) + (η5-6-exo-phenylcyclohexadienyl)manganesetricarbonyl → 5-exo-phenylcyclohexenyltricarbonylmanganese (131414-33-0)

Guidance literature:

In tetrahydrofuran; byproducts: (1-phenylcyclohexenyl)tricarbonylmanganese, (2-phenylcyclohexenyl)tricarbonylmanganese, (4-exo-phenylcyclohexenyl)tricarbonylmanghanese; to stirred soln. in THF added LiAlH4 under N2, after 3 h added water; distd. at 140°C/0.01 Torr;

DOI:10.1016/S0022-328X(00)81031-1

upstream raw materials:

lithium aluminium tetrahydride